NMR in Organometallic Chemistry by Paul S. Pregosin

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NMR in Organometallic Chemistry

Paul S. Pregosin
406 pages
April 2012
The ultimate guide for anyone working in transition organometallic chemistry and related fields.

This book provides the background and practical guidance on how to efficiently work with routine research problems in NMR. It adopts a problem-solving approach with many examples taken from recent literature to show readers how to interpret the data.

Perfect for PhD students, postdocs and other newcomers in organometallic and inorganic chemistry, as well as for organic chemists involved in transition metal catalysis.

Preface XI

Abbreviations XIII

1 Introduction 1

2 Routine Measuring and Relaxation 7

3 COSY and HMQC 2-D Sequences 19

4 Overhauser Effects and 2-D NOESY 39

5 Diffusion Constants via NMR Measurements 55

6 Chemical Shifts 63

7 Coupling Constants 207

8 Dynamics 279

9 Preface to the Problems 311

10 Organometallic Introduction 313

11 NMR Problems 319

12 Solutions to the Problems and Comments 361

Index 389


Paul S. Pregosin received his Ph. D. at the City University of New York. He then carried out postdoctoral research at Queen Mary College, University of London (1970 - 1971), and at the University of Delaware (1971 - 1973). In 1973, he moved to Swiss Federal Institute of Technology in Zurich, Switzerland, where he became Professor of Inorganic Chemistry in 1987. He has also received the Werner Prize
for his work on NMR-spectroscopic studies of transition metal complexes.

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