HPLC: Practical and Industrial Applications, Second Edition By Swadesh

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HPLC: Practical and Industrial Applications, Second Edition

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Features

 

  • Presents highly conceptual information in plain language, making it accessible to students and easy to read for experienced scientists
  • Includes a comprehensive review of HPLC literature, eliminating the need for multiple references
  • Provides extensive indexing and a careful structure to facilitate rapid answers to urgent problems
  • Integrates important non-technical issues with the realities of the workplace, including discussion of a range of topics, from management theory to regulatory considerations and ethicsNew in the Second Edition:
  • Updates of all major topics highlighting recent literature and new developments
  • Expanded discussion of mass spectroscopy, electrophoretic separations, and ultra-micro separations
  • Further discussion on the nature and future of industrial development
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    Summary

    Product specifications, regulatory constraints, and tight production schedules impose considerable pressures on separation scientists in industry. The first edition of HPLC: Practical and Industrial Applications helped eliminate the need for extensive library or laboratory research when confronting a problem, an unfamiliar technique, or work in a new area. Its plain language, comprehensive coverage of separation topics, and practical organization made it an accessible and convenient reference manual for anyone working in or just entering the field. 

    Since its publication in 1997, however, much has changed. The areas of mass spectroscopy, electrophoretic separations, and ultra-micro separations have blossomed, focus on quality control has intensified, and the literature has grown significantly. The Second Edition incorporates all of these changes and more. It is now fully current, with chapter supplements that include updated references and discussions of techniques.

    This book examines analytical HPLC as it is actually used in industry. Whether you are just entering industry, switching from one industry to another, or simply enjoy understanding how things are made, HPLC: Practical and Industrial Applications will help you solve problems and get up to speed in new areas quickly, comfortably, and with a genuine sense of mastery.

     

    TABLE OF CONTENTS :

     

    INTRODUCTION, Jeffrey R. Larson, James E. Tingstad, and Joel K. Swadesh
    Overview
    Pumps
    Columns
    Chromatographic modes
    Detectors
    Chromatographic theory
    Laboratory operations
    The role of laboratory management
    AUTOMATED SAMPLING IN THE PROCESS ENVIRONMENT, Jeffrey R. Larson
    Issues in process HPLC
    Case histories
    Future directions for on-line HPLC process monitors
    Summary
    CHROMATOGRAPHY IN PROCESS DEVELOPMENT, Patricia Puma
    Scope of process chromatography
    Special hardware requirements
    Validation considerations
    Case history
    Summary
    REVERSED PHASE HPLC, Rekha D. Shah and Cynthia A. Maryanoff
    Introduction
    Chromatographic practice in RPLC
    Selected applications
    Case history: optimizing a chemical synthesis by RPLC
    Conclusions
    ION EXCHANGE CHROMATOGRAPHY, Joel K. Swadesh 
    Introduction
    Ion exchange stationary phases
    Electrochemical detectors
    Applications
    Case history: isolation and partial characterization of hementin, a compound of biopharmaceutical interest
    Acknowledgments
    GEL PERMEATION CHROMATOGRAPHY, Rajesh G. Beri, Laurel S. Hacche, and Carl F. Martin
    Introduction
    Detectors for gel permeation chromatography
    Application of aqueous size-exclusion chromatography352 to carbohydrates: a case history
    HIGH PERFORMANCE CAPILLARY ELECTROPHORESIS: AN OVERVIEW, Kálmán Benedik and András Guttman
    Introduction
    Fundamentals
    Instrument
    Separation modes
    Applications
    Conclusions
    Index

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